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Organic Indigo Vat Recipe

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Organic Indigo Vat Recipe

I recently did a natural dye tutorial on creating a organic indigo vat for the lovely folk over at Fabric-store. I decided to talk a little about indigo & share the recipe & process over here for anyone interested. 

Indigo is the name given to the dye that comes from plants (of which there are many species ) containing the indigotin compound which produce an incredible blue dye. Used throughout Asia, South America & Africa, indigo has a rich and vibrant history & is one of the oldest know natural dyes used by man. Woad its  European counterpart, which also contains the dyestuff indigotin, was used throughout France, Germany, England during the late medieval ages. 

Organic indigo vat tutorial

 

The recipe I am sharing is from french chemist & botanist, Micheal Garcia known as the 1-2-3 indigo vat, using as the name suggests three ingredients which are Indigo - Lime - Fructose. 

Before we get into the details let me explain a few things about the ingredients and the creating of the vat. For this recipe, you will need indigo powder which can be purchased in any dye supply store. Indigo comes in many forms such as cakes, paste, powders or granules, not to be confused with synthetically produced indigo. For this recipe, I am using indigo dye powder from indigofera tinctoria (see my recent post on natural dye resources for suppliers in your area ). The lime refers to calcium hydroxide also known as slaked lime, builders lime or hydrated lime ( not to be confused with quick lime or chalk) . Fructose granules can be purchased in health shops or some regular grocery stores (regular sugar does not work, I double checked this myself).

The process of dyeing with indigo is unlike many other natural dyes as it needs a specific type of alkali environment for the indigo dye molecule to be soluble in water. 

Organic indigo vat tutorial

 

From a simplified perspective: when you mix all three of these ingredients together, you create a alkaline environment which allows a chemical reaction takes place that allows the indigo molecule to be released & made available to bind with your fibre. 

Indigo               +            Base/Alkali          +            Reducing Agent    

natural indigo powder  +  calcium hydroxide/slaked lime  +  fructose

For this recipe, I am using 2 tbsp (25g) of indigo, which will dye roughly 2 lbs of fibre light to medium shade.

1 part indigo : 2 parts slaked lime : 3 parts fructose 

For 2tbsp (25g) of indigo, I will need 4 tbsp (50g) of Lime & 6tbsp (75g) of Fructose. 

Measure your ingredients in a 1:2:3 ratio (indigo, lime, fructose). Less indigo will give lighter shades and more indigo will give darker shades. The more items you dye in your vat the more indigo you will need. When first starting, I find it is always best to test with a small amount of indigo so you can practice the process, begin to understand how it works and learn about the shades possibles. Once you have a basic understanding you can go ahead & increase the amount of indigo you use and the pieces you dye. As the indigo powder is not cheap its best to start small and build your way up slowly. 

Organic indigo vat tutorial

 

What you need : 

1 part Indigo 

2 parts Lime

3 parts Fructose

Large glass container ( or plastic if you don’t have glass) to mix Indigo. I used a 1ltr mason jar

Metal Spoon

Wooden Spoon

2 Cups Hot water, more on hand in case you need it 

Non-reactive pot or bucket

Dust Mask 

Gloves

Organic indigo vat tutorial

 

Method:

  1. Measure out your ingredients based on the 1:2:3 ration above. 
  2. Wearing your mask & gloves, you are going to start by making your stock solution, once that is ready you will add your stock to a larger pot of water. 
  3. Add a small amount of water to your mason jar to dissolve your indigo, I have broken a few mason jars by putting hot water straight in. Now I put a small bit of lukewarm water in first before adding very hot water. Add your indigo powder & wet it out to form a paste. Add 8 fl oz of hot water (1 cup) & continue to wet out your indigo by pressing it against the sides of the jar until it is mixed fully with the water. 
  4. Add the lime powder & stir until this is mixed with the indigo solution. If your liquid becomes pasty or thick add more hot water to dissolve. 
  5. When both of those are mixed well, add your fructose and mix fully, again adding more hot water as you need to. At this point, my liquid became very thick and difficult to dissolve but I kept adding small amounts of hot water and continued to mix and press it out until it was completely incorporated. I then added hot water to fill the mason jar to the top & stirred the mixture for another minute, making sure all three ingredients were mixed thoroughly. At this point, my solution was a lovely dark green colour.  
  6. Leave your solution to sit for one hour ( I set a timer on my phone). After one hour stir the solution to mix up and residue on the bottom of the jar, then for the next hour stir every 10-15 minutes. Let it settle for the next hour after which your stock solution will start to separate & have distinguished layers.

Organic indigo vat tutorial Organic indigo vat tutorial

 

How to tell if the stock is ready:

It is ready once it has a layer of coppery scum & blue flower (gathering of blue bubbles) on top. There should be a separation of the liquid from the sludge at the bottom. The liquid should be a yellowish-green or browner in colour. 

Organic indigo vat tutorial

Once your stock is ready: 

  1. Fill a non-reactive pot, container or bucket with hot water. Being very careful, slowly empty your solution with the indigo into the pot of hot water and stir gently. Let it sit for roughly 12-20 minutes.
  2. When your vat becomes yellow-green and there's a blue flower ( dark blue metallic bubbles ) with coppery scum on top, your vat is now ready to use. You can also test by dipping white paper into the solution, the solution should be a yellowy or golden brown. when you remove the paper it should turn from a green to blue once it oxidizes. Your indigo vat is now ready to use. 

Organic indigo vat tutorial

Organic indigo vat tutorial

 

Dyeing with your Vat:

(Make sure to scour your fabric throughly before adding to the vat, there are lots of resources online with detailed instructions on preparing your fabric for dyeing. Always pre-soak your fabric in water for at least 1-2 hours before adding to dye. The depth of shade depends on the type of indigo, vat and number of dips.) 

When working with an indigo vat you must be careful when putting things in & out of the vat as you don't want to introduce too much oxygen into the vat. 

Before you introduce your fabric, remove the flower ( blue bubbly scum ) from the top and set it aside, you will put this back when you are finished working with your vat. 

When introducing fibre to the dye, make sure you do it slowly and carefully, making sure you submerge fully & leaving you fibre in the dye for at least 1 minute longer if possible. 

Slowly remove your items from the vat being careful not to let the liquid splash into the vat. I like to have a drip bowl on hand to collect the excess liquid. Once you remove your fibre, you will see it turn from a green to blue as it oxidizes. 

Only when it has fully oxidised can you dip it back in the vat. The more you dip it the darker your shades will be. For the lightest colours dip 1-2 times. Just remember to let the colour completely change to blue before re-dipping. 

When you are finished dyeing, rinse your fibre fully to remove any excess dye & hang to dry. At this point, you can let it sit for a few days or wash it according to the fibre type. 

Caring for your vat:

You can continue to use your vat until it is "exhausted" or yields little colour at which point it will need more indigo powder. I always like to warm my vat up a little bit if I haven't used it for a while. If you want to start getting into maintaining a vat, you will need to purchase pH strips. An indigo vat likes a pH of between 9-11, if the ph is too low add 1tbsp of lime, dissolve it fully, stir and let it sit. If the pH is too high add 1tbsp fructose, stir and let it sit. I find it is best to keep the solution warm and give it time to rebalance before re-testing the pH. Let it settle for a few hours, when the solution is clear brown, it should be ready to use again. If your vat gets weak and starts to lose colour you can always re-add to it using the 1:2:3 ration above. 

Disposing of your vat:

This solution can be disposed of safely down your drain or added to your compost. You can neutralize the solution by whisking air into the vat. By doing this you are introducing carbon dioxide which reacts with the lime to create calcium carbonate which can be safely disposed of down your drain.